腺苷和蟲(chóng)草素的測(cè)定

編號(hào)：C15000912                                 貨號(hào)：152200542

填料：ATEO-C18                                  流動(dòng)相：乙腈/水=5/95

柱長(zhǎng)：0.25m                                     柱壓：12.5MPa 

內(nèi)徑：4.6mm                                     波長(zhǎng)：260nm 

粒徑：5μm                                      流量：1.0mL/min 

樣品：蛹蟲(chóng)草子實(shí)體粉樣品                        進(jìn)樣體積：10μL 

溫度：35℃                                      適用PH：2-8

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保留時(shí)間     名稱       峰面積       峰分離度     理論塔板數(shù)     峰拖尾因子

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4.889                  556381        4.68         61155           1.06      

7.575                  254524        3.75         48489           0.99      

8.947       腺苷       124970        1.24         46121           1.19      

18.352      蟲(chóng)草素     474951        1.03         55479           0.91      

25.152                 165383        1.24         54056           0.90      

38.722                 341793        0.00         63402           0.92      

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填料：ATEO-C18-AQ                               流動(dòng)相：乙腈/水=5/95

柱長(zhǎng)：0.25m                                     柱壓：16.5MPa 

內(nèi)徑：4.6mm                                     波長(zhǎng)：260nm 

粒徑：5μm                                      流量：1.0mL/min 

樣品：蛹蟲(chóng)草子實(shí)體粉樣品                        進(jìn)樣體積：10μL 

溫度： 35℃                                     適用PH：2-8

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保留時(shí)間         名稱      峰面積       峰分離度    理論塔板數(shù)    峰拖尾因子

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6.672                      200876       3.38        35870          1.15      

7.648          腺苷        87080        17.16       45430          1.10      

14.778         蟲(chóng)草素      395789       9.31        49559          0.94      

20.438                     99522        0.00        60269          0.94      

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